Reaction Blocks: Stirred at -80° to +200°C

We have more than eighteen years of experience in developing and producing temperature- controlled magnetic stirrers. We are committed to continuous improvement which has now led to the development of the VARIOMAG reaction blocks. They allow chemical processes to be modeled elegantly on a small scale.

A New Generation

They have arrived: Our new generation of heated/cooled reaction blocks. The strength of this new generation lies in exactly defined stirring and fast heating to +200°C and - if a cryostat is used - cooling to -80°C.

Our primary objective was to adapt our equipment to satisfy the extended needs now arising in new fields such as combinatorial chemistry. Parallel organic synthesis, materials research, and automation: all these applications are covered by our reaction blocks.

Optional modules such as reflux cooler, thermostats, and inert gas covers further extend the range of possible applications.

But our reaction blocks are not only suitable for solving problems in combinatorial chemistry: the components of this modular system can be optimally adapted to the demands of biotechnology, analytical chemistry, or metallo-organic chemistry. Whether you want to optimize processes, synthesize substances or concentrate samples - you have fond the system you need.

Structure of the
VARIOMAG Reaction Blocks

The new VARIOMAG reaction blocks consist of several modules. This design allows individual variation and maximizes usability, even with frequently changing requirements. Each complete system consists of:

  • VARIOMAG magnetic stirrer
  • Heating/cooling block
  • Reflux cooler
  • Inert gas cover
  • Control unit
    TELEMODUL 40 CT
  • One or two heating/cooling thermostats of your choice
  • Accessories


Reaction block 6.5


Reaction block 48.2 with reflux cooler

VARIOMAG Magnetic Stirrers

The VARIOMAG magnetic stirrers with up to 96 stirring points located below the heating/cooling block stir directly in any stirring vessel. By contrast with conventional magnetic stirrers, they do not use a motor. Variable currents flow through stationary magnetic coils and produce a rotating electromagnetic field. This magnetic drive is completely wear-free, because it does not have any moving parts such as belts, bearings, or motor components. Its hermetically sealed drive resists even aggressive liquids or gases.


Heating/Cooling Block

Fast and cost-effective heating to up to +200°C is made possible by an electrical heater integrated into the aluminum block. To cool samples, the integrated copper coil is simply kept filled with water or a cooling medium. All you have to do is to connect the block to a cold-water pipe or a pump-around cooler. If you use a powerful cryostat, you can obtain block temperatures down to -80°C.

Reflux Cooler

The powerful reflux cooler prevents the evaporation of solvents. It is easy to use and is characterized by high condensation power. The cooling block with its stainless steel frame is a low-maintenance device and ready to use in seconds: just place it on top of the reaction block, and connect it to a cold thermostat or a cold water pipe.


Vacuum Hood

A vacuum hood for concentrating or evaporating samples gently and carefully is available on request.


Heating/cooling block: connections
for up to two cooling circuits

Inert Gas Cover

The inert gas cover prevents the formation of condensate or ice generated by cooling. In addition, inert gas rinses suppress external reactions caused by moisture or oxygen. The inert gas cover fits the block grid and is available in two versions: with silicone membranes (for pipette needles) or with individual covers that close automatically. These covers are required when a robot is used to change samples.


Reaction block 12.2 with
reflux cooler and inert gas cover

Control Unit TELEMODUL 40CT

Each reaction block needs a control unit. The TELEMODUL 40CT digital control unit allows even complex programs to be defined. Required parameters such as speed and temperature are controlled via an operator-friendly menu. Its RS232 computer interface allows several settings such as temperature ramps to be controlled, documented, and archived externally. Because the system is microprocessor controlled, specific customer requirements, such as integration into automated installations, can be accommodated quickly and easily.



3 Frame Sizes

System Options

The modules for your reaction block are available in three frame sizes. There are standard versions for all three sizes, for which the number of stirring points and the bore diameters and depths are fixed. Reaction vessels of other than standard size (cf. table) are adapted to the bore size by using reduction sleeves. However, bore diameters and depths can be modified to accommodate the reaction vessels. The placement of the block bores corresponds to the standard laboratory 96-grid.

Each reaction block consists of a magnetic stirrer, a heating / cooling block with an electrical heater, an integrated cooling circuit, and a control unit. If your samples do not need to be stirred, you can simply order a reaction block without the magnetic stirrer. If you only heat in connection with a thermostat, the electrical heater can be dispensed with. If you want to work with rapid changes in temperature or if you want to operate separate heating and cooling circuits, we can include two copper coils for you.

The well-known and well-proven motorless VARIOMAG magnetic stirrer represents a completely wear-free drive design.

Accessories

Silicone cover protects from ice and dirt

Liquid temperature sensor for control unit TELEMODUL 40CT

Electrical contact thermometer THERMOCONTROL for controlling liquid temperatures

Mounting clamp for THERMOCONTROL

Stainless steel support rod (400 mm long, 12 mm in diameter)

Interface cable (for RS232 interface)

Heating/cooling thermostats on request


Reaction block 24.2 with control unit TELEMODUL and contact thermometer THERMOCONTROL

Magnetic Stirring Bars KOMET

The magnetic stirring bars of the KOMET series were developed specifically for more demanding applications such as stirring highly viscous media. They are made from high-energy magnetic materials and therefore transmit two to three times larger torque loads than conventional stirring bars of comparable size. KOMET 15 and KOMET 30 are particularly well suited for smaller vessels. Stirring disks for test tubes are available as well. The stirring bars cannot be demagnetized by overload or external magnetic fields.


Magnetic stirring bars KOMET

Our modular design was developed with one objective in mind: Maximum utility for a wide range of individual requirements.

Technical Specifications For Standard Versions

Frame 1; Dimensions (WxD): 318 x 418 mm


Reaction block 48.2
with reflux cooler
Reaction block type:

12.5

24.4

48.2

96.1
Number of stirring points:

12 (3x4)

24 (4x6)

48 (6x8)

96 (8x12)
Stirring point distance:

70 mm

55 mm

38 mm

27 mm
Block bore diameter:

57.5 mm

42 mm

25.5 mm

14.5 mm
Block bore depth:

48 mm

78 mm

48 mm

48 mm
Block height:

116 mm

146 mm

116 mm

116 mm
Electrical heating power:

1000W

1000W

1000W

1000W
Order No.:

63101

64101

65101

66101
Reflux cooler:

Click Here For Order Numbers
Inert gas cover:

Click Here For Order Numbers

Frame 2; Dimensions (WxD): 318 x 253 mm


Reaction block 6.5
Reaction block type:

6.5

12.4

24.2

48.1
Number of stirring points:

6(3x2)

12(4x3)

24(6x4)

48(8x6)
Stirring point distance:

70 mm

55 mm

38 mm

27 mm
Block bore diameter:

57.5 mm

42 mm

25.5 mm

14.5 mm
Block bore depth:

48 mm

78 mm

48 mm

48 mm
Block height:

116 mm

146 mm

116 mm

116 mm
Electrical heating power:

530W

530W

530W

530W
Order No.:

62201

63201

64201

65201
Reflux cooler:

Click Here For Order Numbers
Inert gas cover:

Click Here For Order Numbers

Frame 3; Dimensions (WxD): 208 x 253 mm


Reaction block 12.2
Reaction block type:

6.4

12.2

24.1
Number of stirring points:

6(2x3)

12(3x4)

24(4x6)
Stirring point distance:

55 mm

38 mm

27 mm
Block bore diameter:

42 mm

25.5 mm

14.5 mm
Block bore depth:

78 mm

48 mm

48 mm
Block height:

146 mm

116 mm

116 mm
Electrical heating power:

270W

270W

270W
Order No.:

62401

63401

64401
Reflux cooler:

Click Here For Order Numbers
Inert gas cover:

Click Here For Order Numbers

Additional specifications pertaining to all sizes:


3 Frame sizes
Speed:

100 - 2000 rpm
Temperature range:

-80 to +200°C
Nominal stirring power:

4 - 40W
Block material:

AIMgSi1
Frame material:

Stainless steel, enamelled
Electric heater control range:

up to +200°C
Overheat protection:

yes
Heating/cooling thermostat connector:

M16 x 1
Ambient temperature range:

-10 to +56°C at 80% humidity
Protection type (DIN 40050):

IP 31

Technical specifications
for control unit TELEMODUL 40CT


Contact rings
in the reflux cooler

Speed:

100 - 2000 rpm
Constancy of speed:

+/- 3%
Dimensions (WxDxH):

255 x 180 x 90 mm
Weight

3.5 kg
Ambient temperature
at 80% humidity:

0 bis +40°C
Input voltage:

85 - 260V
Frequency:

50 - 60 Hz
Output voltage:

36 VDC
Rated power:

40W
Stirring power (relative to
nominal stirring power):

100 - 10%
Mark of conformity:

Protection class 1, CE mark
IP 20
Max. switchable electrical
heating power:

1000W
Temperature control range:

up to +200°C
Stirring times
(intermittent operation):

1 s - 60 min
Rest times
(intermittent operation):

1 s - 60 min
Interface:

RS232

Magnetic stirring bars KOMET (PTFE coated)
Type:

KOMET 15

KOMET 30

KOMET 16R

KOMET 8S
Dimensions (ø, L):

9 x 15 mm

12 x 30 mm

14 x 8 mm

8 x 4 mm
Order No.:

90715

90730

90714

90708

Order Numbers For VARIOMAG Reaction Blocks

VARIOMAG Reaction Blocks

Block Bore dia.

No. of stirring points

Type 6.5

57.5 mm

6 (3x2)

Order No.

Type 12.5

57.5 mm

12 (3x4)

Order No.

Type 6.4

42 mm

6 (3x2)

Order No.

Type 12.4

42 mm

12 (4x3)

Order No.

Type 24.4

42 mm

24 (4x6)

Order No.
Reaction Block
incl. Control Unit
TELEMODUL 40CT

HP 62 201

HP 63 101

HP 62 401

HP 63 201

HP 64 101
Reflux Cooler
standard

-

-

HP 62 410

HP 63 210

HP 64 110
Reflux Cooler
with contact rings

-

-

HP 62 411

HP 63 211

HP 64 111
Inert Gas Cover
with silicone membranes that can be replaced

HP 62 214

HP 63 114

HP 62 414

HP 63 214

HP 64 114
Inert Gas Cover
with individual covers closing automatically. required when a robot is used to change samples.

HP 62 215

HP 63 115

HP 62 415

HP 63 215

HP 64 115
Spacer Frame

HP 60 225

HP 60 125

HP 60 425

HP 60 225

HP 60 125
Silicone Cover

HP 62 226

HP 63 126

HP 62 426

HP 63 226

HP 64 126
2nd Heating/Cooling Copper Coil-integrated

HP 62 219

HP 63 119

HP 62 419

HP 63 219

HP 64 119

VARIOMAG Reaction Blocks

Block Bore dia.

No. of stirring points

Type 12.2

25.5 mm

12 (3x4)

Order No.

Type 24.2

25.5 mm

24 (6x4)

Order No.

Type 48.2

25.5 mm

48 (6x8)

Order No.

Type 24.1

14.5 mm

24 (4x6)

Order No.

Type 48.1

14.5 mm

48 (8x6)

Order No.

Type 96.1

14.5 mm

96 (8x12)

Order No.
Reaction Block
incl. Control Unit
TELEMODUL 40CT

HP 63 401

HP 64 201

HP 65 101

HP 64 401

HP 65 201

HP 66 101
Reflux Cooler
standard

HP 63 410

HP 64 210

HP 65 110

HP 64 410

HP 65 210

HP 66 110
Reflux Cooler
with contact rings

HP 63 411

HP 64 211

HP 65 111

HP 64 411

HP 65 211

HP 66 111
Inert Gas Cover
with silicone membranes that can be replaced

HP 63 414

HP 64 214

HP 65 114

HP 64 414

HP 65 214

HP 66 114
Inert Gas Cover
with individual covers closing automatically. required when a robot is used to change samples.

HP 63 415

HP 64 215

HP 65 115

HP 64 415

HP 65 215

HP 66 115
Spacer Frame

HP 60 425

HP 60 225

HP 60 125

HP 60 425

HP 60 225

HP 60 125
Silicone Cover

HP 63 426

HP 64 226

HP 65 126

HP 64 426

HP 65 226

HP 66 126
2nd Heating/Cooling Copper Coil-integrated

HP 63 419

HP 64 219

HP 65 119

HP 64 419

HP 65 219

HP 66119

VARIOMAG Reaction Block Accessories

Accessories:

Control Unit TELEMODUL 40CT

External Temperature Probe PT 100

Connecting Cable for external interface (RS 232)

Order No.

HP 90 690

HP 66 151

HP 66 030

Accessories for
Reaction Blocks

Reducing Sleeves
for individual adaptation of the
block bore diameters to vessels with a smaller diameter

from ø, mm
57.5
57.5
42
42
25.5
25.5
14.5

to ø, mm
47
42
25
20
20
16
10

qty/pack
1
1
1
1
1
1
1


HP 66 230
HP 66 231
HP 66 232
HP 66 233
HP 66 234
HP 66 235
HP 66 236

Stirring Bars
Magnetic stirring bars KOMET made of high-energy magnetic material (SmCo, PTFE coated)

KOMET 50 (round shape)
KOMET 30 (round shape)
KOMET 15 (round shape)
KOMET 16R (stand-up ring)
KOMET 8S (stand-up disk)
KOMET 11Q (quarder shape)

format

ø x L
ø x L
ø x L
ø x L
ø x L
[] x L

size - mm

21 x 50
12 x 30
9 x 15
14 x 8
7 x 4
8 x 10

qty/pack

1
1
1
1
1
1

Order No.

HP 90 751
HP 90 730
HP 90 715
HP 90 714
HP 90 708
HP 90 711

We reserve the right to make technical alterations without notice.

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